2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol

Base Information

Chemical Name:2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol
CAS No.:222185-72-0
Molecular Formula:C₄₁H₅₁NO₈
Molecular Weight:685.858
Hs Code.:

Synonyms:2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol

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Chemical Property of 2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol

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Technology Process of 2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol

There total 3 articles about 2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (2S,3R,4R,5R,6S)-8-Azido-2,3,4,6-tetrakis-benzyloxy-octane-1,5-diol

: 222185-72-0
2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol

Guidance literature:: Multi-step reaction with 2 steps

1: NiCl₂*6H₂O-NaBH₄ / ethanol / 0.33 h / Ambient temperature

2: aq. NaHCO₃ / ethyl acetate / 0.25 h

With sodium tetrahydroborate; sodium hydrogencarbonate; nickel dichloride; In ethanol; ethyl acetate;
DOI:10.1016/S0040-4020(98)01218-6

Reference yield:

: 1-O-acetyl 8-azido-2,3,4,6-tetra-O-benzyl-7,8-dideoxy-L-glycero-α(b)-D-gluco-octopyranose

: 222185-72-0
2,3,4,6-tetra-O-benzyl-8-(N-tert-butoxycarbonyl)amino-7,8-dideoxy-L-glycero-D-gluco-octinol

Guidance literature:: Multi-step reaction with 3 steps

1: NaBH₄ / ethanol / 1 h / Heating

2: NiCl₂*6H₂O-NaBH₄ / ethanol / 0.33 h / Ambient temperature

3: aq. NaHCO₃ / ethyl acetate / 0.25 h

With sodium tetrahydroborate; sodium hydrogencarbonate; nickel dichloride; In ethanol; ethyl acetate;
DOI:10.1016/S0040-4020(98)01218-6