(2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

Base Information

Chemical Name:(2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate
CAS No.:1384967-24-1
Molecular Formula:C₃₈H₃₈N₂O₁₇S
Molecular Weight:826.789
Hs Code.:

(2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

Synonyms:(2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

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Chemical Property of (2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

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Technology Process of (2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

There total 1 articles about (2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1045730-24-2
(2S,3S,4S,5R,6R)-2-((benzyloxy)carbonyl)-6-(2,2,2-trichloro-1-iminoethoxy)tetrahydro-2H-pyran-3,4,5-triyl triacetate

: 1384967-23-0
(S)-2-(1-(3-ethoxy-4-hydroxyphenyl)-2-(methylsulfonyl)ethyl)-4-nitroisoindoline-1,3-dione

: 1384967-24-1
(2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -18 - 25 ℃; for 6h; Molecular sieve;

Reference yield:

: 1384967-24-1
(2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

: 1384967-25-2
C₃₁H₃₄N₂O₁₅S

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In ethyl acetate; for 12h; under 1551.49 - 2068.65 Torr;

Reference yield:

: 1384967-24-1
(2S,3S,4S,5R,6S)-2-((benzyloxy)carbonyl)-6-(2-ethoxy-4-((S)-2-(methylsulfonyl)-1-(4-nitro-1,3-dioxoisoindolin-2-yl)ethyl)phenoxy)tetrahydro-2H-pyran-3,4,5-triyltriacetate

: 1384814-90-7
(S)-4-amino-2-[1-(3-ethoxy-4-glucopyranuroxy-phenyl)-2-methanefulfonyl-ethyl]-isoindole-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 12 h / 1551.49 - 2068.65 Torr

2: sodium carbonate / methanol / 2 h / 60 °C

With hydrogen; sodium carbonate; palladium 10% on activated carbon; In methanol; ethyl acetate;