11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine

Base Information

Chemical Name:11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine
CAS No.:133858-18-1
Molecular Formula:C₂₇H₁₉N₃O₂
Molecular Weight:417.467
Hs Code.:

11-acetyl-5-(p-methylphenoxy)-12H-benz-<f>indolo<3,2-b><1,8>naohthyridine

Synonyms:11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine

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Chemical Property of 11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine

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Technology Process of 11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine

There total 3 articles about 11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 16800-68-3
1-acetyl-2,3-dihydro-1H-indol-3-one

: 133858-12-5
3-amino-1-(p-methylphenoxy)isoquinoline-4-carbaldehyde

: 133858-18-1
11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine

Guidance literature:: In ethanol; at 120 ℃; for 3h;

Reference yield:

: 133858-11-4
3-amino-1-(p-methylphenoxy)isoquinoline-4-methanol

: 133858-18-1
11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / manganese dioxide / CHCl₃ / Ambient temperature

2: 22 percent / ethanol / 3 h / 120 °C

With manganese(IV) oxide; In ethanol; chloroform;

Reference yield:

: 125414-83-7
ethyl 3-amino-1-(p-methylphenoxy)isoquinoline-4-carboxylate

: 133858-18-1
11-acetyl-5-(p-methylphenoxy)-12H-benz-indolo<3,2-b><1,8>naohthyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / LiAlH₄ / tetrahydrofuran / 1 h

2: 75 percent / manganese dioxide / CHCl₃ / Ambient temperature

3: 22 percent / ethanol / 3 h / 120 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; In tetrahydrofuran; ethanol; chloroform;