C₁₃H₁₅NO₄

Base Information

• Chemical Name: C₁₃H₁₅NO₄
• CAS No.: 1225228-73-8
• Molecular Formula: C₁₃H₁₅NO₄
• Molecular Weight: 249.266
• Mol file: 1225228-73-8.mol

Synonyms:C₁₃H₁₅NO₄

Chemical Property of C₁₃H₁₅NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₁₃H₁₅NO₄

There total 3 articles about C₁₃H₁₅NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H15NO4 (1225228-68-1) → C13H15NO4 (1225228-73-8) + 1-(3,4-dimethoxyphenyl)ethanone (1131-62-0)

Guidance literature:

With Bacillus coagulans NCIMB 9365; at 30 ℃; for 6h; pH=7; optical yield given as %ee; enantioselective reaction; aq. phosphate buffer; Resolution of racemate;

DOI:10.1016/j.molcatb.2009.12.014

Reference yield:

C13H15NO4 (1225228-68-1) → C13H15NO4 + C13H15NO4 (1225228-73-8) + 1-(3,4-dimethoxyphenyl)ethanone (1131-62-0)

Guidance literature:

With Aspergillus oryzae MIM; at 30 ℃; for 6h; pH=7; optical yield given as %ee; enantioselective reaction; aq. phosphate buffer; Resolution of racemate;

DOI:10.1016/j.molcatb.2009.12.014

Reference yield:

C11H13NO3 (1225228-83-0) + acetic anhydride (108-24-7) → C13H15NO4 (1225228-73-8)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.molcatb.2009.12.014

upstream raw materials:

C₁₃H₁₅NO₄

C₁₁H₁₃NO₃

acetic anhydride