O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate

Base Information

• Chemical Name: O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate
• CAS No.: 130849-46-6
• Molecular Formula: C₂₀H₂₈NO₃P
• Molecular Weight: 361.421
• Mol file: 130849-46-6.mol

Synonyms:O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate

Chemical Property of O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate

There total 3 articles about O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

N-benzyl-(1-methyl-2-phenylethylidene)amine (52189-85-2) + phosphonic acid diethyl ester (762-04-9) → O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate (130849-46-6)

Guidance literature:

at 110 ℃; for 1h;

Reference yield:

1-phenyl-acetone (103-79-7,136675-26-8) → O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate (130849-46-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 62.7 percent / toluene / 2 h / Heating

2: 59 percent / 1 h / 110 °C

In toluene;

Reference yield:

benzylamine (100-46-9) → O,O-diethyl-1-N-benzylamino-1-methyl-2-phenyl-ethyl-phosphonate (130849-46-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 62.7 percent / toluene / 2 h / Heating

2: 59 percent / 1 h / 110 °C

In toluene;

upstream raw materials:

N-benzyl-(1-methyl-2-phenylethylidene)amine

phosphonic acid diethyl ester

benzylamine

1-phenyl-acetone

Downstream raw materials:

O,O-diethyl-1-amino-1-methyl-2-phenyl-ethylphosphonate

1-amino-1-methyl-2-phenyl-ethylphosphonic acid