9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenine

Base Information

• Chemical Name: 9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenine
• CAS No.: 148313-13-7
• Molecular Formula: C₄₈H₄₃N₇O₁₃
• Molecular Weight: 925.909

Synonyms:9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenine

Chemical Property of 9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenine

Chemical Property:

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Technology Process of 9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenine

There total 5 articles about 9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

N6-<2-(4-nitrophenyl)ethoxycarbonyl>-9-<2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>adenine (148313-04-6) + mono-4-methoxytrityl chloride (14470-28-1) → 9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N6-<2-(4-nitrophenyl)ethoxycarbonyl>adenine (148313-13-7)

Guidance literature:

With pyridine; for 24h; Ambient temperature;

DOI:10.1002/hlca.19930760110

Reference yield:

1-methyl-3-[2-(4-nitrophenyl)ethoxycarbonyl]imidazolium chloride (88091-70-7) → 9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N6-<2-(4-nitrophenyl)ethoxycarbonyl>adenine (148313-13-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 91 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h / Ambient temperature

2: 92 percent / AcOH, (Bu₄N)F*3H₂O / tetrahydrofuran / 5 h / Ambient temperature

3: 82 percent / pyridine / 24 h / Ambient temperature

With pyridine; dmap; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1002/hlca.19930760110

Reference yield:

9-[3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-β-D-arabinofuranosyl]adenine (87792-02-7) → 9-<5'-O-(monomethoxytrityl)-2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>-N6-<2-(4-nitrophenyl)ethoxycarbonyl>adenine (148313-13-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 91 percent / 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h / Ambient temperature

2: 92 percent / AcOH, (Bu₄N)F*3H₂O / tetrahydrofuran / 5 h / Ambient temperature

3: 82 percent / pyridine / 24 h / Ambient temperature

With pyridine; dmap; tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; dichloromethane;

DOI:10.1002/hlca.19930760110

upstream raw materials:

N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>-9-<2'-O-<2-(4-nitrophenyl)ethoxycarbonyl>-β-D-arabinofuranosyl>adenine

mono-4-methoxytrityl chloride

1-methyl-3-[2-(4-nitrophenyl)ethoxycarbonyl]imidazolium chloride

9-[3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-1-β-D-arabinofuranosyl]adenine

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