(2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

Base Information

Chemical Name:(2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester
CAS No.:245115-65-5
Molecular Formula:C₁₈H₂₅NO₅
Molecular Weight:335.4
Hs Code.:

Synonyms:(2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

Suppliers and Price of (2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of (2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

There total 3 articles about (2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 115-18-4
2-methyl-3-buten-2-ol

: 83824-81-1
(2S,3S)-3-methylaziridine-1,2-dicarboxylic acid 1-benzylester 2-methyl ester

: 245115-65-5
(2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

Guidance literature:: With boron trifluoride diethyl etherate;
DOI:10.1016/S0040-4039(99)00957-0

Reference yield:

: 74481-56-4
methyl (2S,3S)-N-triphenylmethyl-3-methylaziridine-2-carboxylate

: 245115-65-5
(2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: CF₃COOH / CHCl₃; methanol / 0 °C

1.2: 96 percent / NaHCO₃ / H₂O; ethyl acetate / 20 °C

2.1: 88 percent / BF₃*OEt₂ / 20 °C

With boron trifluoride diethyl etherate; trifluoroacetic acid; In methanol; chloroform; 1.1: Hydrolysis / 1.2: Acylation / 2.1: Ring cleavage;
DOI:10.1021/jo9914566

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 245115-65-5
(2S)-(benzyloxycarbonylamino)-(3R)-(1,1-dimethylallyloxy)butyric acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: CF₃COOH / CHCl₃; methanol / 0 °C

1.2: 96 percent / NaHCO₃ / H₂O; ethyl acetate / 20 °C

2.1: 88 percent / BF₃*OEt₂ / 20 °C

With boron trifluoride diethyl etherate; trifluoroacetic acid; In methanol; chloroform; 1.1: Hydrolysis / 1.2: Acylation / 2.1: Ring cleavage;
DOI:10.1021/jo9914566