C₃₇H₅₂O₃

Base Information

• Chemical Name: C₃₇H₅₂O₃
• CAS No.: 195156-08-2
• Molecular Formula: C₃₇H₅₂O₃
• Molecular Weight: 544.818
• Mol file: 195156-08-2.mol

Synonyms:C₃₇H₅₂O₃

Chemical Property of C₃₇H₅₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₅₂O₃

There total 8 articles about C₃₇H₅₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzaldehyde dimethyl acetal (1125-88-8) → C37H52O3 (195156-08-2)

Guidance literature:

Multi-step reaction with 5 steps

1: CSA / dimethylformamide / Ambient temperature

2: 65 percent / pyridine / 3 h / Ambient temperature

3: pyridine, 4-DMAP / Ambient temperature

4: LiEt₃BH / tetrahydrofuran / Ambient temperature

5: (COCl)2, DMSO, amine base

With pyridine; dmap; oxalyl dichloride; amine base; camphor-10-sulfonic acid; lithium triethylborohydride; dimethyl sulfoxide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(98)00077-8

Reference yield:

soyasapogenol A (508-01-0) → C37H52O3 (195156-08-2)

Guidance literature:

Multi-step reaction with 5 steps

1: CSA / dimethylformamide / Ambient temperature

2: 65 percent / pyridine / 3 h / Ambient temperature

3: pyridine, 4-DMAP / Ambient temperature

4: LiEt₃BH / tetrahydrofuran / Ambient temperature

5: (COCl)2, DMSO, amine base

With pyridine; dmap; oxalyl dichloride; amine base; camphor-10-sulfonic acid; lithium triethylborohydride; dimethyl sulfoxide; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/S0960-894X(98)00077-8

Reference yield:

C37H50O4 (195155-96-5) → C37H52O3 (195156-08-2)

Guidance literature:

Multi-step reaction with 5 steps

1: LiAlH₄ / tetrahydrofuran / 0 - 20 °C

2: 65 percent / pyridine / 3 h / Ambient temperature

3: pyridine, 4-DMAP / Ambient temperature

4: LiEt₃BH / tetrahydrofuran / Ambient temperature

5: (COCl)2, DMSO, amine base

With pyridine; dmap; lithium aluminium tetrahydride; oxalyl dichloride; amine base; lithium triethylborohydride; dimethyl sulfoxide; In tetrahydrofuran;

DOI:10.1016/S0960-894X(98)00077-8

upstream raw materials:

C₃₇H₅₄O₃

benzaldehyde dimethyl acetal

soyasapogenol A

C₃₇H₅₀O₄

Downstream raw materials:

C₃₇H₅₄O₃

C₃₇H₅₄O₃

Refernces