(1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate

Base Information

Chemical Name:(1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate
CAS No.:154704-10-6
Molecular Formula:C₁₉H₂₇NO₅
Molecular Weight:349.427
Hs Code.:

(1R,2R)-Ethyl 2-(benzyloxymethyl)-1-<N-(tert-butoxycarbonyl)amino>cyclopropane-1-carboxylate

Synonyms:(1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate

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Chemical Property of (1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate

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Technology Process of (1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate

There total 7 articles about (1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56552-80-8
(R)-3-benzyloxy-1,2-propanediol

: 154704-10-6
(1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: SOCl₂ / CCl₄

1.2: RuCl₃*3H₂O; NaIO₄ / acetonitrile; H₂O

2.1: NaH / 1,2-dimethoxy-ethane

3.1: LiOH / ethanol

3.2: N₃PO(OPh)2; Et₃N / Heating

With lithium hydroxide; thionyl chloride; sodium hydride; In tetrachloromethane; 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jm070262c

Reference yield:

: 149578-21-2
(S)-4-[(benzyloxy)methyl]-2,2-dioxo-1,3,2-dioxathiolane

: 154704-10-6
(1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / 1,2-dimethoxy-ethane

2.1: LiOH / ethanol

2.2: N₃PO(OPh)2; Et₃N / Heating

With lithium hydroxide; sodium hydride; In 1,2-dimethoxyethane; ethanol;
DOI:10.1021/jm070262c

Reference yield:

: 154704-09-3
(R)-(-)-Diethyl 2-(benzyloxymethyl)cyclopropane-1,1-dicarboxylate

: 154704-10-6
(1R,2R)-Ethyl 2-(benzyloxymethyl)-1-cyclopropane-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: aq. Na₂CO₃ / ethanol / 60 °C

2: NEt₃, diphenylphosphoryl azide / Heating

With diphenylphosphoranyl azide; sodium carbonate; triethylamine; In ethanol;
DOI:10.1055/s-1996-4425