1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone

Base Information

Chemical Name:1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone
CAS No.:1262851-76-2
Molecular Formula:C₂₇H₄₁N₃O
Molecular Weight:423.642
Hs Code.:

Synonyms:1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone

Chemical Property:

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Technology Process of 1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone

There total 6 articles about 1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₅₇N₃O₅

: 1262851-76-2
1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone

Guidance literature:: With chlorotriisopropylsilane; trifluoroacetic acid; In dichloromethane; water; at 20 ℃; for 2h;
DOI:10.1016/j.ejmech.2012.09.048

Reference yield:

: 1202779-00-7
methyl 2-cyano-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}propionate

: 1262851-76-2
1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen / methanol / 120 h / 45 °C

2.1: triethylamine / water; 1,4-dioxane / 18 h / 20 °C / pH 8

3.1: lithium hydroxide; water / 1,4-dioxane / 18 h / 100 °C

4.1: fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

4.2: 168 h / 20 °C

5.1: trifluoroacetic acid; chlorotriisopropylsilane / dichloromethane; water / 2 h / 20 °C

With chlorotriisopropylsilane; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; trifluoroacetic acid; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.09.048

Reference yield:

: 18880-00-7
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene

: 1262851-76-2
1-(2-aminoethylamino)-2-(aminomethyl)-3-[4-(tert-butyl)phenyl]-2-{[4-(tert-butyl)phenyl]methyl}-1-propanone

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 50 °C

2.1: hydrogen / methanol / 120 h / 45 °C

3.1: triethylamine / water; 1,4-dioxane / 18 h / 20 °C / pH 8

4.1: lithium hydroxide; water / 1,4-dioxane / 18 h / 100 °C

5.1: fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C

5.2: 168 h / 20 °C

6.1: trifluoroacetic acid; chlorotriisopropylsilane / dichloromethane; water / 2 h / 20 °C

With chlorotriisopropylsilane; water; hydrogen; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; fluoro-N,N,N',N'-tetramethylformamidinium hexafluorophosphate; trifluoroacetic acid; lithium hydroxide; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.09.048