trans-cyanomethylcarbonylbis(triphenylphosphine)iridium

Base Information

Chemical Name:trans-cyanomethylcarbonylbis(triphenylphosphine)iridium
CAS No.:84206-09-7
Molecular Formula:C₃₉H₃₂IrNOP₂
Molecular Weight:784.857
Hs Code.:

Synonyms:trans-cyanomethylcarbonylbis(triphenylphosphine)iridium

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Chemical Property of trans-cyanomethylcarbonylbis(triphenylphosphine)iridium

Chemical Property:

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Technology Process of trans-cyanomethylcarbonylbis(triphenylphosphine)iridium

There total 2 articles about trans-cyanomethylcarbonylbis(triphenylphosphine)iridium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 84206-08-6
chloroiodo(cyanomethyl)carbonylbis(triphenylphosphine)iridium(III)

: 84206-09-7
trans-cyanomethylcarbonylbis(triphenylphosphine)iridium

Guidance literature:: With tetraethylammonium perchlorate; In acetonitrile; Electrolysis; suspn. of Ir complex in MeCN contg. 0.1 M Et4NClO4 electrolyzed under Ar at -2.0 V vs. Ag/0.1 M Ag(1+) acetonitrile electrode in two-compartment cell on Hg pool electrode; ppt. sepd., washed with cold MeCN, dried in vac.; further crop obtainedby evapn. catholyte in vac. and extn. with benzene followed by addn. oflight petroleum; elem. anal.;
DOI:10.1016/S0022-328X(00)96089-3

Reference yield:

: 85688-70-6
IrH(CO)(PPH₃)3

: 33541-67-2
carbonylhydridotris(triphenylphosphine)iridium(I)

: 84206-09-7
Ir(CO)(CH₂CN)(P(C₆H₅)3)2

Guidance literature:: With MeCN;
DOI:10.1016/S0022-328X(00)98652-2

Reference yield: 80.0%

: 84206-09-7
trans-cyanomethylcarbonylbis(triphenylphosphine)iridium

: 84206-10-0
dioxygen(cyanomethyl)carbonylbis(triphenylphosphine)iridium(III)

Guidance literature:: With oxygen; In benzene; soln. of Ir complex in benzene stirred under O2 (1 atm) for 10 min; hexane added, ppt. recrystd. from benzene/Et2O; elem. anal.;
DOI:10.1016/S0022-328X(00)96089-3