C₃₉H₃₃N₂P₃

Base Information

• Chemical Name: C₃₉H₃₃N₂P₃
• CAS No.: 565238-31-5
• Molecular Formula: C₃₉H₃₃N₂P₃
• Molecular Weight: 622.626
• Mol file: 565238-31-5.mol

Synonyms:C₃₉H₃₃N₂P₃

Chemical Property of C₃₉H₃₃N₂P₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₃₉H₃₃N₂P₃

There total 2 articles about C₃₉H₃₃N₂P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

chloro-diphenylphosphine (1079-66-9,74391-44-9) + diphenylphosphanyl-malononitrile (565238-27-9) → C39H33N2P3 (565238-31-5)

Guidance literature:

diphenylphosphanyl-malononitrile; With [Cp₂ZrHCl]n; In tetrahydrofuran; at -40 - 20 ℃;

chloro-diphenylphosphine; In tetrahydrofuran; for 4h;

DOI:10.1002/ejic.200390128

Reference yield:

chloro-diphenylphosphine (1079-66-9,74391-44-9) → C39H33N2P3 (565238-31-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / 1 h / 0 °C

1.2: 95 percent / tetrahydrofuran / 1 h / 0 - 20 °C

2.1: [Cp₂ZrHCl]n / tetrahydrofuran / -40 - 20 °C

2.2: 54 percent / tetrahydrofuran / 4 h

With [Cp₂ZrHCl]n; lithium diisopropyl amide; In tetrahydrofuran;

DOI:10.1002/ejic.200390128

Reference yield: 81.0%

C39H33N2P3 (565238-31-5) → C39H33N2P3S3

Guidance literature:

With sulfur; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/ejic.200390128

upstream raw materials:

chloro-diphenylphosphine

diphenylphosphanyl-malononitrile