methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate

Base Information

• Chemical Name: methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate
• CAS No.: 377732-35-9
• Molecular Formula: C₂₂H₂₉NO₄S
• Molecular Weight: 403.543

Synonyms:methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate

Chemical Property of methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate

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Technology Process of methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate

There total 2 articles about methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

methyl c-5-[5-(4-methylbenzoylamino)-6-oxoheptyl]-2-methyl-1,3-dioxane-r-2-carboxylate (880080-65-9) → methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate (377732-35-9)

Guidance literature:

With 2,4-bis(methylthio)-1,3-dithia-2,4-diphosphetane-2,4-disulfide; In tetrahydrofuran; at 55 - 75 ℃; for 6h;

DOI:10.1016/j.bmc.2007.10.007

Reference yield:

4-(4-chlorobutyl)-5-ethyl-2-(p-tolyl)oxazole (377732-82-6) + methyl c-5-[5-(4-methylbenzoylamino)-6-oxoheptyl]-2-methyl-1,3-dioxane-r-2-carboxylate (880080-65-9) + 2,4-bis(methylthio)-1,3-dithia-2,4-diphosphetane-2,4-disulfide (82737-61-9) → methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate (377732-35-9)

Guidance literature:

In tetrahydrofuran; ethyl acetate;

Reference yield: 84.0%

methyl 2-methyl-c-5-{4-[5-methyl-2-(4-methylphenyl)-1,3-thiazol-4-yl]butyl}-1,3-dioxane-r-2-carboxylate (377732-35-9) → C21H27NO4S (377732-03-1)

Guidance literature:

With sodium hydroxide; In methanol; water; Heating;

DOI:10.1016/j.bmc.2007.10.007

upstream raw materials:

4-(4-chlorobutyl)-5-ethyl-2-(p-tolyl)oxazole

methyl c-5-[5-(4-methylbenzoylamino)-6-oxoheptyl]-2-methyl-1,3-dioxane-r-2-carboxylate

2,4-bis(methylthio)-1,3-dithia-2,4-diphosphetane-2,4-disulfide

Downstream raw materials:

C₂₁H₂₇NO₄S

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