N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester
CAS No.:5616-82-0
Molecular Formula:C₂₀H₂₈N₂O₅
Molecular Weight:376.453
Hs Code.:

Synonyms:N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

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Chemical Property of N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

Chemical Property:

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Technology Process of N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

There total 2 articles about N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101644-79-5
α-tert-butyl N-(benzyloxycarbonyl)-N-methylglycinate

: 5616-82-0
N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

2: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00097a003

Reference yield:

: 5616-81-9
sarcosine tert-butyl ester

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 5616-82-0
N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at -10 ℃; Yield given;
DOI:10.1021/ja00085a002

Reference yield:

: 5616-82-0
N-(benzyloxycarbonyl)prolylsarcosine tert-butyl ester

: 158629-40-4
N-(benzyloxycarbonyl)-D-phenylalaninylprolylsarcosine tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / 2 h / 760 Torr

2: dicyclohexylcarbodiimide / CH₂Cl₂ / 3 h / -10 °C

With hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00097a003