1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide

Base Information

Chemical Name:1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide
CAS No.:1047991-10-5
Molecular Formula:C₃₅H₄₆N₂O₄
Molecular Weight:558.761
Hs Code.:

Synonyms:1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide

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Chemical Property of 1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide

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Technology Process of 1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide

There total 4 articles about 1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1047990-79-3
2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-2-(pent-4-enoylamido)-N-(1,1,3,3-tetramethylbutyl)-D-galacto-hexonamide

: 1047991-10-5
1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide

Guidance literature:: With water; iodine; In tetrahydrofuran; for 0.5h;
DOI:10.1002/ejoc.201200923

Reference yield:

: 909870-16-2
(3R,4S,5R)-3,4-di-O-benzyl-5-(benzyloxymethyl)-1-pyrroline

: 1047991-10-5
1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide

Guidance literature:: Multi-step reaction with 2 steps

1: indium(III) chloride / acetonitrile / 20 h / 0 - 5 °C / Inert atmosphere

2: water; iodine / tetrahydrofuran / 0.5 h

With indium(III) chloride; water; iodine; In tetrahydrofuran; acetonitrile; 1: |Ugi Condensation;
DOI:10.1002/ejoc.201200923

Reference yield:

: 909870-15-1
2,3,5-tri-O-benzyl-4-deoxy-4-azido-D-lyxose

: 1047991-10-5
1,1,3,3-tetramethylbutyl 2-amino-2,5-anhydro-3,4,6-tri-O-benzyl-2-deoxy-D-galacto-hexonamide

Guidance literature:: Multi-step reaction with 3 steps

1: trimethylphosphane / methanol; toluene / 3 h / 0 °C / Inert atmosphere

2: indium(III) chloride / acetonitrile / 20 h / 0 - 5 °C / Inert atmosphere

3: water; iodine / tetrahydrofuran / 0.5 h

With indium(III) chloride; water; iodine; trimethylphosphane; In tetrahydrofuran; methanol; toluene; acetonitrile; 2: |Ugi Condensation;
DOI:10.1002/ejoc.201200923