1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide

Base Information

Chemical Name:1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide
CAS No.:776313-45-2
Molecular Formula:C₁₅H₁₄F₂O₂S₂
Molecular Weight:328.404
Hs Code.:

Synonyms:1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide

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Technology Process of 1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide

There total 2 articles about 1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 5535-48-8
PVS

: 78031-08-0
[(bromodifluoromethyl)sulfanyl]benzene

: 776313-45-2
1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 10h; Heating;
DOI:10.1021/jo0489768

Reference yield:

: 108-98-5
thiophenol

: 776313-45-2
1,1-difluoro-3-phenylsulfonylpropyl phenyl sulfide

Guidance literature:: Multi-step reaction with 2 steps

1.1: NaH / dimethylformamide / 0.5 h / 20 °C

1.2: 69 percent / dimethylformamide / 3.5 h / -60 °C

2.1: 49 percent / n-Bu₃SnH; AIBN / benzene / 10 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; sodium hydride; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo0489768