1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane

Base Information

Chemical Name:1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane
CAS No.:240131-61-7
Molecular Formula:C₂₄H₃₂N₂O₆S
Molecular Weight:476.594
Hs Code.:

Synonyms:1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane

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Chemical Property of 1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane

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Technology Process of 1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane

There total 3 articles about 1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 46912-02-1
4-(1,1,3,3-tetramethylbutyl)-2-nitrophenol

: 240131-56-0
2-<2-nitrophenyl(thio)ethoxy>ethyl chloride

: 240131-61-7
1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(99)00430-5

Reference yield:

: 4875-10-9
o-nitrothiophenol

: 240131-61-7
1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / dimethylformamide / 6 h / Heating

2: 85 percent / SOCl₂, pyridine / 1 h / 60 °C

3: 84 percent / K₂CO₃ / dimethylformamide

With pyridine; thionyl chloride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(99)00430-5

Reference yield:

: 240131-55-9
2-<2-<2-nitrophenyl(thio)>ethoxy>ethanol

: 240131-61-7
1-<2-nitrophenyl(thio)>-5-<4-(1,1,3,3-tetramethylbutyl)-2-nitrophenoxy>-3-oxapentane

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / SOCl₂, pyridine / 1 h / 60 °C

2: 84 percent / K₂CO₃ / dimethylformamide

With pyridine; thionyl chloride; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(99)00430-5