(Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon

Base Information

Chemical Name:(Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon
CAS No.:74503-50-7
Molecular Formula:C₁₇H₁₀Cl₄N₄O₄
Molecular Weight:476.103
Hs Code.:

Synonyms:(Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon

Suppliers and Price of (Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon

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Technology Process of (Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon

There total 2 articles about (Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 74503-46-1
(Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal

: 119-26-6
(2,4-dinitro-phenyl)-hydrazine

: 74503-50-7
(Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon

Guidance literature:: With sulfuric acid; In ethanol; at 0 ℃; for 1h;

Reference yield:

: 71284-93-0
(Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienoylchlorid

: 74503-50-7
(Z)-2,3,5,5-Tetrachlor-4-phenyl-2,4-pentadienal-2,4-dinitrophenylhydrazon

Guidance literature:: Multi-step reaction with 2 steps

1: 1) ethylenimine, Et₃N, 2) LiAlH₄ / 1) ether, -30 deg C, 30 min, 2) ether, -95 deg C, 2 h

2: 88 percent / H₂SO₄ / ethanol / 1 h / 0 °C

With lithium aluminium tetrahydride; sulfuric acid; 1-ethyleneimine; triethylamine; In ethanol;