Technology Process of C24H31N3O5S
There total 6 articles about C24H31N3O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,4-dioxane; water;
at 100 ℃;
for 3h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2011.12.018
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene / 16 h / 22 °C
2.1: dichloromethane / 16 h / 22 °C
3.1: sodium tetrahydroborate / ethanol / 3 h / 22 °C
3.2: 4 h / Reflux
4.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / 1,4-dioxane; water / 3 h / 100 °C / Inert atmosphere
With
sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,4-dioxane; ethanol; dichloromethane; water; toluene;
2.1: Wittig reaction / 4.1: Suzuki coupling;
DOI:10.1016/j.tetlet.2011.12.018
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: dichloromethane / 16 h / 22 °C
2.1: sodium tetrahydroborate / ethanol / 3 h / 22 °C
2.2: 4 h / Reflux
3.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / 1,4-dioxane; water / 3 h / 100 °C / Inert atmosphere
With
sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,4-dioxane; ethanol; dichloromethane; water;
1.1: Wittig reaction / 3.1: Suzuki coupling;
DOI:10.1016/j.tetlet.2011.12.018
