MSX-196

Base Information

Chemical Name:MSX-196
CAS No.:898194-41-7
Molecular Formula:C₁₈H₁₇FN₄
Molecular Weight:308.358
Hs Code.:

Synonyms:MSX-196

Suppliers and Price of MSX-196

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of MSX-196

Chemical Property:

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Technology Process of MSX-196

There total 3 articles about MSX-196 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 348-54-9
2-Fluoroaniline

: 405175-13-5
4-((pyrimidin-2-ylamino)methyl)benzaldehyde

: 898194-41-7
MSX-196

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 20 ℃;
DOI:10.1021/jm100786g

Reference yield:

: 897657-96-4
(4-((pyrimidin-2-ylamino)methyl)phenyl)methanol

: 898194-41-7
MSX-196

Guidance literature:: Multi-step reaction with 2 steps

1: Dess-Martin periodane / dichloromethane / 1.17 h / 0 - 20 °C

2: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

With sodium tris(acetoxy)borohydride; Dess-Martin periodane; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm100786g

Reference yield:

: 623-27-8
terephthalaldehyde,

: 898194-41-7
MSX-196

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / 1,2-dichloro-ethane / 0.33 h / 20 °C / Molecular sieve

1.2: 24 h / 20 °C / Molecular sieve; Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 1.17 h / 0 - 20 °C

3.1: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

With sodium tris(acetoxy)borohydride; Dess-Martin periodane; acetic acid; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/jm100786g