C₅₆H₅₁N₇Zn

Base Information

Chemical Name:C₅₆H₅₁N₇Zn
CAS No.:952190-07-7
Molecular Formula:C₅₆H₅₁N₇Zn
Molecular Weight:887.458
Hs Code.:

C<sub>56</sub>H<sub>51</sub>N<sub>7</sub>Zn

Synonyms:C₅₆H₅₁N₇Zn

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Chemical Property of C₅₆H₅₁N₇Zn

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Technology Process of C₅₆H₅₁N₇Zn

There total 3 articles about C₅₆H₅₁N₇Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1215310-68-1
C₅₆H₅₃N₅Zn

: 952190-07-7
C₅₆H₅₁N₇Zn

Guidance literature:: With tert.-butylnitrite; trimethylsilylazide; In tetrahydrofuran; at 0 ℃; Inert atmosphere;
DOI:10.1021/ja906020e

Reference yield: 71.0%

: 4648-54-8
trimethylsilylazide

: 1215310-68-1
5,10,15-tris(4-tert-butylphenyl)-20-(4-aminophenyl)porphyrin

: 952190-07-7
5,10,15-tris(4-tert-butylphenyl)-20-(4-azidophenyl)porphyrin

Guidance literature:: With tert.-butylnitrite; In tetrahydrofuran; addn. of tert-butylnitrite and (CH3)3SiN3 to soln. of zinc compd. in C4H8O at 0°C under Ar, stirring for 30 min, for completion addn. of 2 equiv. of tert-butylnitrite, (CH3)3SiN3 (control by thin layer chromy.); Tetrahedron Lett., 2007, 48, 6518; addn. of water, extn. with CH2Cl2, organic phase filtration through hydrophobic filter, evapn., chromy. (toluene);
DOI:10.1021/ja906020e