4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose

Base Information

• Chemical Name: 4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose
• CAS No.: 1413011-48-9
• Molecular Formula: C₇₀H₆₀O₁₉
• Molecular Weight: 1205.24

Synonyms:4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose

Chemical Property of 4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose

Chemical Property:

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Technology Process of 4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose

There total 1 articles about 4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1,2-O-bis(3,5-di-O-allyl-4-O-benzylgalloyl)-4,6-O-anisylidene-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose (1413011-52-5) → 4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose (1413011-48-9)

Guidance literature:

With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dichloro-ethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ol302845n

Reference yield:

4,6-O-anisylidene-1,2-O-bis(4-O-benzylgalloyl)-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose (1413011-48-9) → 4,6-O-anisylidene-3-O-(3,4,5-tri-O-benzylgalloyl)-1,2-[4,4',6,6'-tetrahydroxy-5,5'-bisbenzyloxy-1,1'-biphenyl-2,2'-dicarboxylate]-β-D-glucopyranose (1413011-54-7)

Guidance literature:

With N-butylamine; copper dichloride; In methanol; at 20 ℃; Inert atmosphere;

DOI:10.1021/ol302845n

upstream raw materials:

1,2-O-bis(3,5-di-O-allyl-4-O-benzylgalloyl)-4,6-O-anisylidene-3-O-(3,4,5-tri-O-benzylgalloyl)-β-D-glucopyranose

Downstream raw materials:

4,6-O-anisylidene-3-O-(3,4,5-tri-O-benzylgalloyl)-1,2-[4,4',6,6'-tetrahydroxy-5,5'-bisbenzyloxy-1,1'-biphenyl-2,2'-dicarboxylate]-β-D-glucopyranose

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