(R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester

Base Information

Chemical Name:(R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester
CAS No.:720707-61-9
Molecular Formula:C₅₅H₇₄O₄Si₂
Molecular Weight:855.361
Hs Code.:

Synonyms:(R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester

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Technology Process of (R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester

There total 2 articles about (R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 13487-46-2
arachidonyl alcohol

: (R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid

: 720707-61-9
(R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2004.03.093

Reference yield:

: 720707-69-7
benzyl {(R)-2,3-di-[(t-butyldiphenylsilyl)oxy]}propionate

: 720707-61-9
(R)-2,3-di-[(t-butyldiphenylsilyl)oxy]propionic acid icosa-5,8,11,14-tetraenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / H₂ / Pd/C / tetrahydrofuran / 72 h

2: 57 percent / DCC; DMAP / CH₂Cl₂ / 20 °C

With dmap; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2004.03.093