Technology Process of C32H36F3N3O5S
There total 17 articles about C32H36F3N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 3h;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-iodo-succinimide / tetrahydrofuran; acetonitrile / 0.17 h / Inert atmosphere; Sealed tube
1.2: 5 h / 20 °C / Inert atmosphere; Sealed tube
2.1: boron tribromide / dichloromethane / 4.16 h / -78 - 20 °C / Inert atmosphere; Sealed tube
3.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere; Sealed tube
3.2: 1 h / 0 - 20 °C / Inert atmosphere; Sealed tube
4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; 1,2-dimethoxyethane / 3 h / 90 °C / Inert atmosphere; Sealed tube
With
pyridine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium(0); boron tribromide; potassium carbonate;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: dmap / acetonitrile / 0.17 h / 0 °C / Inert atmosphere; Sealed tube
1.2: 2.5 h / 0 - 20 °C / Inert atmosphere; Sealed tube
2.1: lithium hydroxide monohydrate / water / 2 h / 0 - 20 °C / Inert atmosphere; Sealed tube
3.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere; Sealed tube
4.1: ammonium acetate / toluene / 5 h / 110 °C / Inert atmosphere; Sealed tube
5.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere; Sealed tube
6.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; 1,2-dimethoxyethane / 3 h / 90 °C / Inert atmosphere; Sealed tube
With
dmap; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; lithium hydroxide monohydrate; ammonium acetate; potassium acetate; potassium carbonate; triethylamine;
In
1,2-dimethoxyethane; dichloromethane; water; toluene; acetonitrile;