(1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester

Base Information

• Chemical Name: (1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester
• CAS No.: 76097-51-3
• Molecular Formula: C₂₀H₂₇NO₄
• Molecular Weight: 345.439

Synonyms:(1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester

Chemical Property of (1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester

Chemical Property:

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Technology Process of (1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester

There total 2 articles about (1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

benzyl chloroformate (501-53-1,94274-21-2) + (1'S,4'R,6'R)-3'-Azabicyclo<4.4.0>decan-4'-essigsaeure-methylester-hydrochlorid → (1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester (76097-51-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 3h;

DOI:10.1002/hlca.19800630507

Reference yield:

→ (1'S,4'R,6'R)-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester + (1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester (76097-51-3)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol; at 72 ℃; for 6h; Yield given. Yields of byproduct given;

DOI:10.1002/hlca.19800630507

Reference yield:

potassium tert-butylate (865-47-4) + (1'S,4'R,6'R)-3'-benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-methylester (76097-51-3) → (1'S,4'R,6'R)-Benzyloxycarbonyl-3'-azabicyclo<4.4.0>decan-4'-essigsaeure-t-butylester + (3S,4aR,8aS)-3-tert-Butoxycarbonylmethyl-octahydro-isoquinoline-2-carboxylic acid benzyl ester

Guidance literature:

In tert-butyl alcohol; at 72 ℃; for 6h; Yield given. Yields of byproduct given;

DOI:10.1002/hlca.19800630507

upstream raw materials:

benzyl chloroformate

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