2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole

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Chemical Name:2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole
CAS No.:1251827-20-9
Molecular Formula:C₂₈H₄₅NO₄S₂Si₂
Molecular Weight:579.973
Hs Code.:

Synonyms:2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole

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Chemical Property of 2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole

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Technology Process of 2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole

There total 1 articles about 2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: C₂₈H₄₅NO₂S₂Si₂

: 1251827-20-9
2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole

Guidance literature:: With hexaammonium heptamolybdate tetrahydrate; dihydrogen peroxide; In ethanol; water; at 0 - 20 ℃; for 3h;

Reference yield: 17.0%

: 1251827-03-8
(1R,3αR,7αR)-7α-methyl-1-((R)-1-(triethylsilyloxy)propan-2-yl)hexahydro-1H-inden-4(2H)-one

: 1251827-20-9
2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole

: 1251827-18-5
((1R,3R)-5-((E)-2-((1R,3αS,7αR)-7α-methyl-1-((R)-1-(triethylsilyloxy)propan-2-yl)dihydro-1H-inden-4(2H,5H,6H,7H,7αH)-ylidene)ethylidene)-2-methylenecyclohexane-1,3-diyl)bis(oxy)bis(tert-butyldimethylsilane)

Guidance literature:: (1R,3αR,7αR)-7α-methyl-1-((R)-1-(triethylsilyloxy)propan-2-yl)hexahydro-1H-inden-4(2H)-one; 2-(2-((3R,5R)-3,5-bis(tertbutyldimethylsilyloxy)-4-methylenecyclohexylidene)ethylsulfonyl)benzo[d]thiazole; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With sodium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃; for 18h;