tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate

Base Information

Chemical Name:tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate
CAS No.:1352879-24-3
Molecular Formula:C₂₁H₂₇NO₆
Molecular Weight:389.448
Hs Code.:

Synonyms:tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate

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Chemical Property of tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate

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Technology Process of tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate

There total 2 articles about tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1065515-11-8
1-methoxy-4-((1E,3E)-4-nitrobuta-1,3-dienyl)benzene

: 84109-76-2
tert-butyl 2-oxocyclopentanecarboxylate

: 1352879-24-3
tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate

Guidance literature:: With C₃₁H₅₀N₄O; In ethyl acetate; at -15 ℃; for 32h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.200901337

Reference yield: 78.0%

: 4995-06-6
4-Nitro-1-(4-methoxy-phenyl)-butadien-(1,3)

: 84109-76-2
tert-butyl 2-oxocyclopentanecarboxylate

: 1352879-24-3
tert-butyl (R)-1-[(S,E)-1'-nitro-4'-(4''-methoxyphenyl)but-3'-en-2'-yl]-2-oxocyclopentanecarboxylate

Guidance literature:: With C₂₆H₃₀N₂O₂; In dichloromethane; at 20 ℃; for 96h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/adsc.201100618