C₆₆H₇₉N₅O₈

Base Information

Chemical Name:C₆₆H₇₉N₅O₈
CAS No.:1354327-82-4
Molecular Formula:C₆₆H₇₉N₅O₈
Molecular Weight:1070.38
Hs Code.:

C<sub>66</sub>H<sub>79</sub>N<sub>5</sub>O<sub>8</sub>

Synonyms:C₆₆H₇₉N₅O₈

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Chemical Property of C₆₆H₇₉N₅O₈

Chemical Property:

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Technology Process of C₆₆H₇₉N₅O₈

There total 12 articles about C₆₆H₇₉N₅O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53008-62-1,53008-61-0
2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl iodide

: 1354327-80-2
C₃₂H₄₅N₅O₃

: 1354327-82-4
C₆₆H₇₉N₅O₈

Guidance literature:: C₃₂H₄₅N₅O₃; With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In benzene; at 65 ℃; for 0.166667h; Inert atmosphere; Molecular sieve;

2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl iodide; In benzene; at 65 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ml200278u

Reference yield:

: 1354327-71-1
C₄₀H₃₆O₅

: 1354327-82-4
C₆₆H₇₉N₅O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / 3 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 4 h / 120 °C / Inert atmosphere; Microwave irradiation

4.1: toluene-4-sulfonic acid / methanol / 5 h / 20 °C / Inert atmosphere

5.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / benzene / 0.17 h / 65 °C / Inert atmosphere; Molecular sieve

5.2: 3 h / 65 °C / Inert atmosphere

With sodium azide; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ml200278u

Reference yield:

: 131645-01-7
C₁₁H₂₆N₂

: 1354327-82-4
C₆₆H₇₉N₅O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol / 3 h / 20 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

3.1: sodium azide / N,N-dimethyl-formamide / 4 h / 120 °C / Inert atmosphere; Microwave irradiation

4.1: toluene-4-sulfonic acid / methanol / 5 h / 20 °C / Inert atmosphere

5.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / benzene / 0.17 h / 65 °C / Inert atmosphere; Molecular sieve

5.2: 3 h / 65 °C / Inert atmosphere

With sodium azide; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ml200278u