methyl 2-formyl-5-o-octylbenzoate

Base Information

Chemical Name:methyl 2-formyl-5-o-octylbenzoate
CAS No.:1265287-01-1
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:methyl 2-formyl-5-o-octylbenzoate

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Chemical Property of methyl 2-formyl-5-o-octylbenzoate

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Technology Process of methyl 2-formyl-5-o-octylbenzoate

There total 6 articles about methyl 2-formyl-5-o-octylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₃₀O₄

: 1265287-01-1
methyl 2-formyl-5-o-octylbenzoate

Guidance literature:: With sulfuric acid; water; In tetrahydrofuran; at 20 ℃; for 15h;

Reference yield:

: 118-90-1
ortho-methylbenzoic acid

: 1265287-01-1
methyl 2-formyl-5-o-octylbenzoate

Guidance literature:: Multi-step reaction with 7 steps

1.1: bromine; iron / 16 h / 0 - 20 °C

1.2: 15 h / Reflux

2.1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 15 h / Reflux

3.1: water; silver nitrate / isopropyl alcohol / 20 °C / Darkness

4.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 16 h / 100 °C

5.1: ammonium chloride / methanol / 16 h / Reflux

6.1: palladium on carbon; hydrogen / ethanol / 3 h / 20 °C / 760.05 Torr

7.1: sulfuric acid; water / tetrahydrofuran / 15 h / 20 °C

With N-Bromosuccinimide; sulfuric acid; palladium on carbon; water; hydrogen; bromine; palladium diacetate; iron; ammonium chloride; silver nitrate; triethylamine; tris-(o-tolyl)phosphine; dibenzoyl peroxide; In tetrahydrofuran; methanol; tetrachloromethane; ethanol; N,N-dimethyl-formamide; isopropyl alcohol; 4.1: Heck reaction;

Reference yield:

: 1016163-89-5
methyl 5-bromo-2- formylbenzoate

: 1265287-01-1
methyl 2-formyl-5-o-octylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 16 h / 100 °C

2: ammonium chloride / methanol / 16 h / Reflux

3: palladium on carbon; hydrogen / ethanol / 3 h / 20 °C / 760.05 Torr

4: sulfuric acid; water / tetrahydrofuran / 15 h / 20 °C

With sulfuric acid; palladium on carbon; water; hydrogen; palladium diacetate; ammonium chloride; triethylamine; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; 1: Heck reaction;