trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate

Base Information

Chemical Name:trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate
CAS No.:335672-99-6
Molecular Formula:C₂₅H₂₉N₅O₄S₂
Molecular Weight:527.668
Hs Code.:

Synonyms:trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate

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Chemical Property of trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate

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Technology Process of trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate

There total 3 articles about trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 72-14-0
Sulfathiazole

: 335672-84-9
N-butyl-N-[2-(methacryloyloxy)ethyl]aniline

: 335672-99-6
trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate

Guidance literature:: Sulfathiazole; With hydrogenchloride; acetic acid; sodium nitrite;

N-butyl-N-[2-(methacryloyloxy)ethyl]aniline; In hydrogenchloride; 2-methoxy-ethanol; acetic acid;

Reference yield:

: 122-98-5
2-Anilinoethanol

: 335672-99-6
trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 53 percent / KI / ethanol / 35 h / Heating

2.1: 4-(dimethylamino)pyridine; pyridine; BHT / 0.25 h / Heating

3.1: aq. HCl; AcOH; NaNO₂

3.2: 93 percent / 2-methoxy-ethanol; aq. HCl; acetic acid

With pyridine; hydrogenchloride; dmap; 2,6-di-tert-butyl-4-methyl-phenol; acetic acid; potassium iodide; sodium nitrite; In ethanol;

Reference yield:

: 3046-94-4
N-butyl-N-(2-hydroxyethyl)aniline

: 335672-99-6
trans-2-n-butyl-2-[4-({4-[(1,3-thiazol-2-ylamino)sulfonyl]phenyl}diazenyl)phenylamino]ethyl methacrylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-(dimethylamino)pyridine; pyridine; BHT / 0.25 h / Heating

2.1: aq. HCl; AcOH; NaNO₂

2.2: 93 percent / 2-methoxy-ethanol; aq. HCl; acetic acid

With pyridine; hydrogenchloride; dmap; 2,6-di-tert-butyl-4-methyl-phenol; acetic acid; sodium nitrite;