NbCl₅*FCH₂CN

Base Information

• Chemical Name: NbCl₅*FCH₂CN
• CAS No.: 33726-49-7
• Molecular Formula: C₂H₂Cl₅FNNb
• Molecular Weight: 329.214
• Mol file: 33726-49-7.mol

Synonyms:NbCl₅*FCH₂CN

Chemical Property of NbCl₅*FCH₂CN

Chemical Property:

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Technology Process of NbCl₅*FCH₂CN

There total 1 articles about NbCl₅*FCH₂CN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

fluoroacetonitrile (503-20-8) + niobium pentachloride (10026-12-7) → NbCl5*FCH2CN (33726-49-7)

Guidance literature:

In dichloromethane; reaction with excess FCH2CN at 30°C;; evaporation of solvent in N2 atmosphere at 120-150 Torr, drying at 5E-2 Torr for 5 -10 hours;;

DOI:10.1002/hlca.19710540818

upstream raw materials:

fluoroacetonitrile

niobium pentachloride