5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

Base Information

Chemical Name:5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole
CAS No.:118683-69-5
Molecular Formula:C₂₁H₂₂N₄O₃
Molecular Weight:378.431
Hs Code.:

Synonyms:5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

Suppliers and Price of 5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

Chemical Property:

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Technology Process of 5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

There total 4 articles about 5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 118684-29-0
4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamonitrile

: 118683-69-5
5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 120 ℃; for 48h;

Reference yield:

: 1866-39-3,940-61-4
trans-p-methylcinnamic acid

: 118683-69-5
5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

Guidance literature:: Multi-step reaction with 4 steps

1: 2) DMF / 1) CH₂Cl₂, reflux, 1 h, 2) 0 deg C, 30 min

2: 77 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 0.5 h / Heating; Irradiation

3: 43 percent / K₂CO₃ / acetone / 18 h / Heating

4: 17 percent / NaN₃, NH₄Cl / dimethylformamide / 48 h / 120 °C

With N-Bromosuccinimide; sodium azide; Perbenzoic acid; potassium carbonate; ammonium chloride; N,N-dimethyl-formamide; In tetrachloromethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 28446-70-0
(E)-4-methylcinnamonitrile

: 118683-69-5
5-<4-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>cinnamyl>-1H-tetrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / N-bromosuccinimide, benzoyl peroxide / CCl₄ / 0.5 h / Heating; Irradiation

2: 43 percent / K₂CO₃ / acetone / 18 h / Heating

3: 17 percent / NaN₃, NH₄Cl / dimethylformamide / 48 h / 120 °C

With N-Bromosuccinimide; sodium azide; Perbenzoic acid; potassium carbonate; ammonium chloride; In tetrachloromethane; N,N-dimethyl-formamide; acetone;