C₂₅H₃₀O₇

Base Information

Chemical Name:C₂₅H₃₀O₇
CAS No.:1600522-93-7
Molecular Formula:C₂₅H₃₀O₇
Molecular Weight:442.509
Hs Code.:

C<sub>25</sub>H<sub>30</sub>O<sub>7</sub>

Synonyms:C₂₅H₃₀O₇

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Chemical Property of C₂₅H₃₀O₇

Chemical Property:

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Technology Process of C₂₅H₃₀O₇

There total 5 articles about C₂₅H₃₀O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 619-44-3
methyl 4-iodobenzoate

: 1600522-27-7
C₁₇H₂₂O₅

: 1600522-93-7
C₂₅H₃₀O₇

Guidance literature:: methyl 4-iodobenzoate; With isopropylmagnesium bromide; lithium chloride; In tetrahydrofuran; at -25 ℃; for 0.5h; Inert atmosphere;

C₁₇H₂₂O₅; In tetrahydrofuran; at -30 ℃; for 1h; Inert atmosphere;
DOI:10.1002/anie.201308824

Reference yield:

: 1428369-29-2
C₂₇H₃₆O₃Si

: 1600522-93-7
C₂₅H₃₀O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.17 h / -78 °C / Inert atmosphere

2.1: tetrahydrofuran / 19 h / -78 - 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

5.1: lithium chloride; isopropylmagnesium bromide / tetrahydrofuran / 0.5 h / -25 °C / Inert atmosphere

5.2: 1 h / -30 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; isopropylmagnesium bromide; Dess-Martin periodane; lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201308824

Reference yield:

: 1600522-88-0
C₃₃H₄₂O₅Si

: 1600522-93-7
C₂₅H₃₀O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

2.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere

3.1: lithium chloride; isopropylmagnesium bromide / tetrahydrofuran / 0.5 h / -25 °C / Inert atmosphere

3.2: 1 h / -30 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; isopropylmagnesium bromide; Dess-Martin periodane; lithium chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201308824