(2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine

Base Information

Chemical Name:(2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine
CAS No.:914618-60-3
Molecular Formula:C₂₇H₂₇NO₄
Molecular Weight:429.516
Hs Code.:

Synonyms:(2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine

Chemical Property:

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Technology Process of (2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine

There total 1 articles about (2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: benzyl N-(2-benzyloxy-1-p-methoxyphenylbut-3-enyl)carbamate

: 914618-60-3
(2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / NaH / tetrahydrofuran; dimethylformamide; various solvent(s) / 1 h / 20 °C

2: 82 percent / first-generation Grubbs catalyst / CH₂Cl₂ / 4 h / 20 °C

With sodium hydride; Grubbs catalyst first generation; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2007.01.028

Reference yield: 83.0%

: 914618-60-3
(2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine

: 914618-61-4
(2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)piperidine

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; at 20 ℃; for 0.5h;
DOI:10.1016/j.tet.2007.01.028

Reference yield:

: 914618-60-3
(2S,3S)-1-benzyloxycarbonyl-(3-benzyloxy-2-p-methoxyphenyl)-1,2,3,6-tetrahydropyridine

: 3-benzyloxy-piperidine-1,2-dicarboxylic acid 1-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / H₂ / PtO₂ / methanol / 0.5 h / 20 °C

2: NaIO₄ / RuCl₃ / H₂O; acetonitrile; ethyl acetate / 4 h / 20 °C

With sodium periodate; hydrogen; platinum(IV) oxide; ruthenium trichloride; In methanol; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.tet.2007.01.028