Technology Process of C23H28N2O2
There total 3 articles about C23H28N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,2-dimethoxyethane; water;
at 80 ℃;
for 27h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: thionyl chloride; N,N-dimethyl-formamide / 1 h / 20 - 70 °C / Cooling with ice
2: pyridinium p-toluenesulfonate / tetrahydrofuran / 16 h / 20 °C
3: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; 1,2-dimethoxyethane / 27 h / 80 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); thionyl chloride; pyridinium p-toluenesulfonate; potassium carbonate; N,N-dimethyl-formamide;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: pyridinium p-toluenesulfonate / tetrahydrofuran / 16 h / 20 °C
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; 1,2-dimethoxyethane / 27 h / 80 °C / Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); pyridinium p-toluenesulfonate; potassium carbonate;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;