6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine

Base Information

• Chemical Name: 6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine
• CAS No.: 76381-68-5
• Molecular Formula: C₂₆H₃₄N₈O₈
• Molecular Weight: 586.605

Synonyms:6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine

Chemical Property of 6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine

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Technology Process of 6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine

There total 1 articles about 6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.5%

Boc-Phe(p-NO2)-OH (33305-77-0) + 3'-amino-3'-deoxy-N6,N6-dimethyladenosine (58-60-6) → 6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine (76381-68-5)

Guidance literature:

With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 20h; Ambient temperature;

DOI:10.1021/jm00135a013

Reference yield: 88.3%

6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine (76381-68-5) → 6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine (76494-20-7)

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; for 4h; under 760 Torr; Ambient temperature;

DOI:10.1021/jm00135a013

Reference yield: 67.0%

6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine (76381-68-5) → 6-(dimethylamino)-9-<3'-<(p-nitro-L-phenylalanyl)amino>-3'-deoxy-β-D-ribofuranosyl>purine (76381-77-6)

Guidance literature:

With trifluoroacetic acid; for 0.133333h; Ambient temperature;

DOI:10.1021/jm00135a013

upstream raw materials:

Boc-Phe(p-NO₂)-OH

3'-amino-3'-deoxy-N⁶,N⁶-dimethyladenosine

Downstream raw materials:

6-(dimethylamino)-9-<3'-<(p-nitro-L-phenylalanyl)amino>-3'-deoxy-β-D-ribofuranosyl>purine

6-(dimethylamino)-9-<3'-<amino>-3'-deoxy-β-D-ribofuranosyl>purine

(S)-2-Amino-3-(4-amino-phenyl)-N-[(2S,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-hydroxymethyl-tetrahydro-furan-3-yl]-propionamide

(S)-3-(4-Acetylamino-phenyl)-2-amino-N-[(2S,3S,4R,5R)-5-(6-dimethylamino-purin-9-yl)-4-hydroxy-2-hydroxymethyl-tetrahydro-furan-3-yl]-propionamide

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