C₄₂H₅₃N₃O₈S

Base Information

Chemical Name:C₄₂H₅₃N₃O₈S
CAS No.:1354551-67-9
Molecular Formula:C₄₂H₅₃N₃O₈S
Molecular Weight:759.964
Hs Code.:

C<sub>42</sub>H<sub>53</sub>N<sub>3</sub>O<sub>8</sub>S

Synonyms:C₄₂H₅₃N₃O₈S

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Chemical Property of C₄₂H₅₃N₃O₈S

Chemical Property:

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Technology Process of C₄₂H₅₃N₃O₈S

There total 10 articles about C₄₂H₅₃N₃O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1354551-61-3
C₃₅H₄₇N₃O₆

: 98-59-9
p-toluenesulfonyl chloride

: 1354551-67-9
C₄₂H₅₃N₃O₈S

Guidance literature:: With trimethylamine hydrochloride; triethylamine; In dichloromethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.10.045

Reference yield:

: 872346-84-4
benzyl (3S,4S)-3-hydroxy-4-methyloctanoate

: 1354551-67-9
C₄₂H₅₃N₃O₈S

Guidance literature:: Multi-step reaction with 7 steps

1: dmap; diisopropyl-carbodiimide / dichloromethane; water / 30 h / 0 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

5: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C

6: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

7: trimethylamine hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; dmap; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; hydrogen; trimethylamine hydrochloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; diisopropyl-carbodiimide; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.045

Reference yield:

: 1354551-64-6
(3S,4S)-3-(Boc-D-Chg-O)-4-methyloctanoic acid

: 1354551-67-9
C₄₂H₅₃N₃O₈S

Guidance literature:: Multi-step reaction with 5 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 5 h / 0 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / ethanol / 3 h / 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane; water / 1 h / 20 °C

4: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 72 h / 0 - 20 °C / Inert atmosphere

5: trimethylamine hydrochloride; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

With hydrogenchloride; 1-hydroxy-7-aza-benzotriazole; palladium 10% on activated carbon; hydrogen; trimethylamine hydrochloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.10.045