(nitridotetrabromo technetate(VI))AsPh₄

Base Information

Chemical Name:(nitridotetrabromo technetate(VI))AsPh₄
CAS No.:95012-28-5
Molecular Formula:Br₄NTc*C₂₄H₂₀As
Molecular Weight:814.874
Hs Code.:

(nitridotetrabromo technetate(VI))AsPh<sub>4</sub>

Synonyms:(nitridotetrabromo technetate(VI))AsPh₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (nitridotetrabromo technetate(VI))AsPh₄

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Technology Process of (nitridotetrabromo technetate(VI))AsPh₄

There total 1 articles about (nitridotetrabromo technetate(VI))AsPh₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: sodium azide

: 34035-97-7
ammonium pertechnetate

: 507-28-8,14842-08-1
tetraphenylarsonium chloride

: 95012-28-5
(nitridotetrabromo technetate(VI))AsPh₄

Guidance literature:: With HBr; In water; The mixt. of Tc-compound, conc. HBr, and NaN3 in water was heated underreflux for 20 min, Ph4AsCl in H2O was added;; filtered, washed with conc. HBr, then Et2O, recrystd. from CH3CN; elem.anal.;;
DOI:10.1039/DT9840002395

Reference yield: 80.0%

: 95012-28-5
(nitridotetrabromo technetate(VI))AsPh₄

: 507-28-8,14842-08-1
tetraphenylarsonium chloride

: {(Ph₄As)2}tetrakis(isothiocyanato)nitridotechnetate(V)

Guidance literature:: With potassium thioacyanate; In acetone; a saturated soln. of KSCN added to a soln. of Tc-complex; a soln. of As-compound added; filtered; added isopropanol; pptd.; recrystd. from acetone/isopropanol; elem. anal.;

Reference yield: 78.0%

: 95012-28-5
(nitridotetrabromo technetate(VI))AsPh₄

: (nitridoperoxobromo technetate(VII))AsPh₄

Guidance literature:: With H₂O₂; In acetonitrile; H2O2 is added to a soln. of the Tc-compd. in the minimum volume of CH3CN; Mixt. is reduced in volume on a rotary evaporator, ppt. is collected by filtration, washed with water, and dried under vac., elem. anal.;
DOI:10.1016/S0020-1693(00)85079-3