C₂₂H₂₈O₇

Base Information

Chemical Name:C₂₂H₂₈O₇
CAS No.:1375645-03-6
Molecular Formula:C₂₂H₂₈O₇
Molecular Weight:404.46
Hs Code.:

C<sub>22</sub>H<sub>28</sub>O<sub>7</sub>

Synonyms:C₂₂H₂₈O₇

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Chemical Property of C₂₂H₂₈O₇

Chemical Property:

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Technology Process of C₂₂H₂₈O₇

There total 5 articles about C₂₂H₂₈O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1375645-31-0
C₂₄H₃₂O₇

: 1375645-03-6
C₂₂H₂₈O₇

Guidance literature:: C₂₄H₃₂O₇; With sodium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran; methanol; water; at 20 ℃;
DOI:10.1016/j.tetlet.2012.03.098

Reference yield:

: 1375645-24-1
3-bromomethyl-4-iodofuran

: 1375645-03-6
C₂₂H₂₈O₇

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 0 - 20 °C

1.2: 2 h / 70 °C

2.1: dmap; water; sodium chloride / dimethyl sulfoxide / 19 h / 180 °C

3.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / dichloromethane / 0.5 h / 20 °C

3.2: 1 h / 80 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

5.1: sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 20 °C

5.2: 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; sodium hydride; sodium chloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 2.1: Krapcho decarboalkoxylation / 3.2: Stille coupling;
DOI:10.1016/j.tetlet.2012.03.098

Reference yield:

: 1375645-09-2
3-(β-gem-dicarbethoxy)ethyl-4-iodofuran

: 1375645-03-6
C₂₂H₂₈O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap; water; sodium chloride / dimethyl sulfoxide / 19 h / 180 °C

2.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / dichloromethane / 0.5 h / 20 °C

2.2: 1 h / 80 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

4.1: sodium hydroxide / tetrahydrofuran; methanol; water / 1 h / 20 °C

4.2: 20 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; tetrabutyl ammonium fluoride; water; tri-n-butyl-tin hydride; sodium chloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; 1.1: Krapcho decarboalkoxylation / 2.2: Stille coupling;
DOI:10.1016/j.tetlet.2012.03.098