trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester

Base Information

Chemical Name:trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester
CAS No.:552289-50-6
Molecular Formula:C₂₀H₃₅F₃O₄SSi
Molecular Weight:456.642
Hs Code.:

Synonyms:trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester

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Chemical Property of trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester

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Technology Process of trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester

There total 1 articles about trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 145100-51-2
N-(5-chloropyridin-2-yl)-1,1,1-trifluoro-N-[(trifluoromethyl)sulphonyl]methanesulphonamide

: (5S)-2-methyl-5-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohex-2-enone

: 552289-50-6
trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester

Guidance literature:: (5S)-2-methyl-5-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohex-2-enone; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

N-(5-chloropyridin-2-yl)-1,1,1-trifluoro-N-[(trifluoromethyl)sulphonyl]methanesulphonamide; In tetrahydrofuran; at -78 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jo9010156

Reference yield: 76.0%

: 552289-50-6
trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester

: 552289-38-0
(2S)-{2-[1(R)-3-iodo-4-methylcyclohexa-2,4-dienyl]propoxy}triisopropylsilane

Guidance literature:: trifluoromethanesulfonic acid (3R)-6-methyl-3-[1(S)-methyl-2-(triisopropylsilyloxy)ethyl]cyclohexa-1,5-dienyl ester; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; hexamethyldistannane; lithium chloride; In tetrahydrofuran; at 23 - 70 ℃; Inert atmosphere;

With N-iodo-succinimide; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo9010156