C₃₅H₃₁N₂O₈P

Base Information

Chemical Name:C₃₅H₃₁N₂O₈P
CAS No.:1478097-91-4
Molecular Formula:C₃₅H₃₁N₂O₈P
Molecular Weight:638.613
Hs Code.:

C<sub>35</sub>H<sub>31</sub>N<sub>2</sub>O<sub>8</sub>P

Synonyms:C₃₅H₃₁N₂O₈P

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Chemical Property of C₃₅H₃₁N₂O₈P

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Technology Process of C₃₅H₃₁N₂O₈P

There total 12 articles about C₃₅H₃₁N₂O₈P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1477517-11-5
C₁₆H₁₄BrN₂O₆P

: 4-benzyloxy-5-methoxy-7-methyl-1-naphthylboronic acid

: 1478097-91-4
C₃₅H₃₁N₂O₈P

Guidance literature:: With potassium phosphate; C₂₂H₂₉O₃P; palladium diacetate; In water; toluene; at 30 - 35 ℃; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja409669r

Reference yield:

: 73311-51-0
1-methoxy-3-methyl-1-trimethylsilyloxy-1,3-butadiene

: 1478097-91-4
C₃₅H₃₁N₂O₈P

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloromethane / 20 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: sodium dithionite dihydrate / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

3.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

4.2: 20 °C / Inert atmosphere

5.1: potassium hydroxide / methanol / 3 h / 50 °C / Inert atmosphere

5.2: 20 °C / pH 5 - 6 / Inert atmosphere

6.1: triethylamine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

7.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene / 1,4-dioxane / 7 h / 100 °C / Inert atmosphere

8.1: sodium periodate / tetrahydrofuran; water / 0.5 h / 20 °C

8.2: 12 h / 20 °C

9.1: C₂₂H₂₉O₃P; palladium diacetate; potassium phosphate / water; toluene / 30 - 35 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; sodium periodate; sodium dithionite dihydrate; C₂₂H₂₉O₃P; potassium acetate; palladium diacetate; sodium hydride; triethylamine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 1.1: |Diels-Alder Cycloaddition / 1.2: |Diels-Alder Cycloaddition / 7.1: |Suzuki-Miyaura Coupling / 9.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ja409669r

Reference yield:

: 924-50-5
Methyl 3,3-dimethylacrylate

: 1478097-91-4
C₃₅H₃₁N₂O₈P

Guidance literature:: Multi-step reaction with 10 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: 0.5 h / -78 °C

2.1: dichloromethane / 20 h / 20 °C

2.2: 0.5 h / 20 °C

3.1: sodium dithionite dihydrate / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

6.1: potassium hydroxide / methanol / 3 h / 50 °C / Inert atmosphere

6.2: 20 °C / pH 5 - 6 / Inert atmosphere

7.1: triethylamine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8.1: potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 1,1'-bis-(diphenylphosphino)ferrocene / 1,4-dioxane / 7 h / 100 °C / Inert atmosphere

9.1: sodium periodate / tetrahydrofuran; water / 0.5 h / 20 °C

9.2: 12 h / 20 °C

10.1: C₂₂H₂₉O₃P; palladium diacetate; potassium phosphate / water; toluene / 30 - 35 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; sodium periodate; sodium dithionite dihydrate; C₂₂H₂₉O₃P; potassium acetate; palladium diacetate; sodium hydride; triethylamine; potassium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2.1: |Diels-Alder Cycloaddition / 2.2: |Diels-Alder Cycloaddition / 8.1: |Suzuki-Miyaura Coupling / 10.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ja409669r