C₄₃H₆₈O₁₀Si₂

Base Information

Chemical Name:C₄₃H₆₈O₁₀Si₂
CAS No.:153145-47-2
Molecular Formula:C₄₃H₆₈O₁₀Si₂
Molecular Weight:801.178
Hs Code.:

C<sub>43</sub>H<sub>68</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₃H₆₈O₁₀Si₂

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Chemical Property of C₄₃H₆₈O₁₀Si₂

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Technology Process of C₄₃H₆₈O₁₀Si₂

There total 19 articles about C₄₃H₆₈O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 108-24-7
acetic anhydride

: 153145-44-9
C₄₁H₆₆O₉Si₂

: 153145-47-2
C₄₃H₆₈O₁₀Si₂

Guidance literature:: With pyridine; dmap; at 25 ℃; for 24h;

Reference yield:

: 153145-26-7
C₃₂H₅₆O₇Si₂

: 153145-47-2
C₄₃H₆₈O₁₀Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

2: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

3: 95 percent / CH₂Cl₂ / 15 h / -45 °C

4: 63 percent / Burgess' reagent

5: 100 percent / pyridine

6: 65 percent / OsO₄

7: DBU / toluene / 2 h / 105 °C

8: 75 percent / pyridine, DMAP / 24 h / 25 °C

With pyridine; dmap; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane; toluene;

Reference yield:

: 153145-20-1
C₃₄H₅₈O₇Si₂

: 153145-47-2
C₄₃H₆₈O₁₀Si₂

Guidance literature:: Multi-step reaction with 15 steps

1: O₃

2: KMnO₄, KH₂PO₄

4: 93 percent / LDA / tetrahydrofuran / 0.5 h / -78 °C

5: 100 percent / p-TsOH

6: 92 percent / PhSK / dimethylformamide / 3 h / 86 °C

7: acid

8: 92 percent / EtN(i-Pr)2, (Bu)4NI / CH₂Cl₂ / 32 h / Heating

9: 1.) LDA, 2.) mCPBA / 1.) THF, -78 deg C, 2.) hexane, 25 deg C, 5 h

10: 95 percent / CH₂Cl₂ / 15 h / -45 °C

11: 63 percent / Burgess' reagent

12: 100 percent / pyridine

13: 65 percent / OsO₄

14: DBU / toluene / 2 h / 105 °C

15: 75 percent / pyridine, DMAP / 24 h / 25 °C

With pyridine; dmap; potassium permanganate; potassium dihydrogenphosphate; osmium(VIII) oxide; Burgess Reagent; tetra-(n-butyl)ammonium iodide; (2E)-3-(4-hydroxyphenyl-3-methoxyphenyl)-1-phenylprop-2-en-1-one; toluene-4-sulfonic acid; ozone; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene;