benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside
CAS No.:85065-35-6
Molecular Formula:C₃₅H₃₄N₂O₁₃
Molecular Weight:690.661
Hs Code.:

Synonyms:benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside

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Chemical Property of benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside

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Technology Process of benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside

There total 8 articles about benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.7%

: 85071-06-3
benzyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-6-O-(3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-β-D-glucopyranoside

: 85065-35-6
benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 0 ℃;
DOI:10.1016/0008-6215(83)88321-9

Reference yield:

: 7772-87-4
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl chloride

: 85065-35-6
benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: 79.3 percent / mercury(II) cyanide / nitromethane; toluene / 20 °C / 4 Angstroem molecular sieve

2: 90.2 percent / sodium methoxide / methanol / 4 h

3: pyridine / Ambient temperature

4: pyridine / 24 h / Ambient temperature

5: 67.2 percent / silver perchlorate / nitromethane / Ambient temperature; 4 Angstroem molecular sieve

6: 92.7 percent / sodium methoxide / methanol; CHCl₃ / 4 h / 0 - 4 °C

With pyridine; sodium methylate; silver perchlorate; mercury(II) cyanide; In methanol; nitromethane; chloroform; toluene;

Reference yield:

: 80035-32-1
benzyl 2-deoxy-2-phthalimido-β-D-glucopyranoside

: 85065-35-6
benzyl 2-deoxy-6-O-(2-deoxy-2-phthalimido-β-D-glucopyranosyl)-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / Ambient temperature

2: pyridine / 24 h / Ambient temperature

3: 67.2 percent / silver perchlorate / nitromethane / Ambient temperature; 4 Angstroem molecular sieve

4: 92.7 percent / sodium methoxide / methanol; CHCl₃ / 4 h / 0 - 4 °C

With pyridine; sodium methylate; silver perchlorate; In methanol; nitromethane; chloroform;