5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate

Base Information

Chemical Name:5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate
CAS No.:1609584-76-0
Molecular Formula:C₂₉H₂₃N₄*ClO₄
Molecular Weight:526.979
Hs Code.:

Synonyms:5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate

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Technology Process of 5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate

There total 1 articles about 5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 3435-51-6
4-ethenylbenzonitrile

: 1,3,4-triphenyl-4H-1,2,4-triazol-1-ium perchlorate

: 1609584-76-0
5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; at 80 ℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique; Sealed tube;
DOI:10.1021/ol501256d

Reference yield:

: 100-43-6,329041-72-7
4-vinylpyridine

: 1609584-76-0
5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate

: 1609584-90-8
(E)-4-(4-(pyridin-4-yl)but-1-en-1-yl)benzonitrile

: 1609585-02-5
(E)-4-(4-(pyridin-4-yl)but-3-en-1-yl)benzonitrile

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; at 160 ℃; for 16h; Overall yield = 63 %; Overall yield = 14.7 mg; Inert atmosphere; Glovebox; Schlenk technique; Sealed tube;
DOI:10.1021/ol501256d

Reference yield:

: 10537-63-0
1-(4-vinylphenyl)ethanone

: 1609584-76-0
5-(2-(4-cyanophenyl)ethyl)-1,3,4-triphenyl-1H-1,2,4-triazol-4-ium perchlorate

: 1609584-86-2
(E)-4-(4-(4-acetylphenyl)but-1-en-1-yl)benzonitrile

: (E)-4-(4-(4-acetylphenyl)but-3-en-1-yl)benzonitrile

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; at 160 ℃; for 16h; Overall yield = 56 %; Overall yield = 15.6 mg; Inert atmosphere; Glovebox; Schlenk technique; Sealed tube;
DOI:10.1021/ol501256d