(1E)-1-(dec-3-en-2-ylidene)-2-(2,4-dinitrophenyl)hydrazine

Base Information

• Chemical Name: (1E)-1-(dec-3-en-2-ylidene)-2-(2,4-dinitrophenyl)hydrazine
• CAS No.: 3013-10-3
• Molecular Formula: C₁₆H₂₂N₄O₄
• Molecular Weight: 334.375
• Mol file: 3013-10-3.mol

Synonyms:3-Decen-2-one,(2,4-dinitrophenyl)hydrazone (7CI,8CI); NSC 230197

Chemical Property of (1E)-1-(dec-3-en-2-ylidene)-2-(2,4-dinitrophenyl)hydrazine

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 456.141°C at 760 mmHg
• Flash Point: 229.666°C
• Density: 1.194g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1E)-1-(dec-3-en-2-ylidene)-2-(2,4-dinitrophenyl)hydrazine

There total 8 articles about (1E)-1-(dec-3-en-2-ylidene)-2-(2,4-dinitrophenyl)hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,4-dinitro-phenyl)-hydrazine (119-26-6) → trans--methyl-keton-2,4-dinitrophenylhydrazon (3013-10-3)

Guidance literature:

With hydrogenchloride;

DOI:10.1177/0148607101025004219

Reference yield:

heptanal (111-71-7) → trans--methyl-keton-2,4-dinitrophenylhydrazon (3013-10-3)

Guidance literature:

Multi-step reaction with 3 steps

1: aqueous NaOH-solution

2: aqueous phosphoric acid; copper / 150 °C

3: aqueous methanol. HCl

With hydrogenchloride; sodium hydroxide; phosphoric acid; copper;

DOI:10.1177/0148607101025004219

Reference yield:

dec-3-yn-2-one (91658-50-3) → trans--methyl-keton-2,4-dinitrophenylhydrazon (3013-10-3)

Guidance literature:

Multi-step reaction with 2 steps

1: palladium/calcium carbonate; ethanol / Hydrogenation

2: aqueous methanol. HCl

With hydrogenchloride; palladium on activated charcoal; Lindlar's catalyst; ethanol;

DOI:10.1177/0148607101025004219

upstream raw materials:

dec-3-en-2-one

(2,4-dinitro-phenyl)-hydrazine

n-heptan1ol

dec-3c-en-2-one