phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:225242-46-6
Molecular Formula:C₂₄H₂₃NO₈S
Molecular Weight:485.515
Hs Code.:

Synonyms:phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 5 articles about phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 79528-49-7
phenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 225242-46-6
phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With Candida rugosa lipase immobilized on octadecyl-Sepabeads; In aq. phosphate buffer; acetonitrile; at 20 ℃; for 24h; Reagent/catalyst; regioselective reaction; Inert atmosphere; Enzymatic reaction;
DOI:10.1002/ejoc.201900382

Reference yield:

: 1322656-53-0
C₄₃H₃₇NO₈S

: 225242-46-6
phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With acetic acid; In water; at 50 ℃; for 3h;
DOI:10.1016/j.carres.2011.03.029

Reference yield:

: 10022-13-6,31505-44-9,79733-86-1,81704-02-1,116347-84-3,131234-07-6,144300-04-9
1,3,4,6-tetra-O-acetyl-2-phthalimido-2-deoxy-α-D-glucopyranose

: 108-98-5
thiophenol

: 225242-46-6
phenyl 3,4-di-O-acetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere

2: Candida rugosa lipase immobilized on octadecyl-Sepabeads / aq. phosphate buffer; acetonitrile / 24 h / 20 °C / Inert atmosphere; Enzymatic reaction

With boron trifluoride diethyl etherate; Candida rugosa lipase immobilized on octadecyl-Sepabeads; In aq. phosphate buffer; dichloromethane; acetonitrile;
DOI:10.1002/ejoc.201900382