C₂₀H₂₆S₆

Base Information

• Chemical Name: C₂₀H₂₆S₆
• CAS No.: 72444-33-8
• Molecular Formula: C₂₀H₂₆S₆
• Molecular Weight: 458.822
• Mol file: 72444-33-8.mol

Synonyms:C₂₀H₂₆S₆

Chemical Property of C₂₀H₂₆S₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₀H₂₆S₆

There total 8 articles about C₂₀H₂₆S₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C20H24S6(2+)*2I(1-) → C20H26S6 (72444-33-8)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; at -78 ℃;

Reference yield:

4,4'-(p-Phenylen)dibutyrylchlorid (54622-13-8) → C20H26S6 (72444-33-8)

Guidance literature:

Multi-step reaction with 7 steps

1: diethyl ether

2: NaCl, HCl / methanol

3: 89 percent / acetone / 0.5 h / Heating

4: 70percent HClO₄ / CHCl₃; diethyl ether

5: P₄S₁₀ / xylene / 2.5 h / 140 °C

6: nitromethane / 2.5 h / 70 °C

7: 91 percent / NaBH₄ / tetrahydrofuran; methanol / -78 °C

With hydrogenchloride; sodium tetrahydroborate; perchloric acid; tetraphosphorus decasulfide; sodium chloride; In tetrahydrofuran; methanol; diethyl ether; nitromethane; chloroform; acetone; xylene;

Reference yield:

4-[4-(3-carboxypropyl)phenyl]butyric acid (22339-62-4) → C20H26S6 (72444-33-8)

Guidance literature:

Multi-step reaction with 8 steps

1: 83 percent / SOCl₂ / 2 h / 90 °C

2: diethyl ether

3: NaCl, HCl / methanol

4: 89 percent / acetone / 0.5 h / Heating

5: 70percent HClO₄ / CHCl₃; diethyl ether

6: P₄S₁₀ / xylene / 2.5 h / 140 °C

7: nitromethane / 2.5 h / 70 °C

8: 91 percent / NaBH₄ / tetrahydrofuran; methanol / -78 °C

With hydrogenchloride; sodium tetrahydroborate; thionyl chloride; perchloric acid; tetraphosphorus decasulfide; sodium chloride; In tetrahydrofuran; methanol; diethyl ether; nitromethane; chloroform; acetone; xylene;

upstream raw materials:

4,4'-(p-Phenylen)dibutyrylchlorid

4-[4-(3-carboxypropyl)phenyl]butyric acid

1,4-bis-(5'-chloro-4'-oxopentyl)-benzene

C₁₈H₁₈O₂S₄