syn-α,4'-dibromoacetophenone oxime

Base Information

• Chemical Name: syn-α,4'-dibromoacetophenone oxime
• CAS No.: 1236132-56-1
• Molecular Formula: C₈H₇Br₂NO
• Molecular Weight: 292.958

Synonyms:syn-α,4'-dibromoacetophenone oxime

Chemical Property of syn-α,4'-dibromoacetophenone oxime

Chemical Property:

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Technology Process of syn-α,4'-dibromoacetophenone oxime

There total 1 articles about syn-α,4'-dibromoacetophenone oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-bromophenacyl bromide (99-73-0,132309-76-3) → syn-α,4'-dibromoacetophenone oxime (1236132-56-1) + anti-α,4'-dibromoacetophenone oxime (71426-51-2)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; at 20 ℃; for 24h;

DOI:10.1080/10426501003769728

Reference yield: 83.0%

1-methylindole (603-76-9) + syn-α,4'-dibromoacetophenone oxime (1236132-56-1) → (E)-1-(p-bromophenyl)-2-(1-methyl-1H-indol-3-yl)ethanoneoxime

Guidance literature:

With sodium carbonate; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1007/s00706-016-1763-1

Reference yield: 72.0%

3-Methylindole (83-34-1) + syn-α,4'-dibromoacetophenone oxime (1236132-56-1) → 3-(p-bromophenyl)-4a-methyl-4,4a,9,9a-tetrahydro[1,2]oxazine[6,5-b]indole

Guidance literature:

With sodium carbonate; In dichloromethane; at 20 ℃; for 91h;

DOI:10.1007/s00706-016-1763-1

upstream raw materials:

para-bromophenacyl bromide

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