Technology Process of 8a-phenyl-Δ4,4a-octahydroquinoline
There total 6 articles about 8a-phenyl-Δ4,4a-octahydroquinoline which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuric acid;
In
dichloromethane;
for 5h;
Ambient temperature;
DOI:10.1021/jm00087a020
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 32 percent / O2 / ethyl acetate / Ambient temperature
2: 64 percent / diethyl ether / 2 h / Heating
3: 91 percent / conc. H2SO4 / CH2Cl2 / 5 h / Ambient temperature
With
sulfuric acid; oxygen;
In
diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jm00087a020
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 87 percent / dioxane / 1.5 h / Heating
2: LiAlH4 / diethyl ether / 0.5 h / Ambient temperature
3: aq. NaOH / 1 h / 100 °C
4: 32 percent / O2 / ethyl acetate / Ambient temperature
5: 64 percent / diethyl ether / 2 h / Heating
6: 91 percent / conc. H2SO4 / CH2Cl2 / 5 h / Ambient temperature
With
sodium hydroxide; lithium aluminium tetrahydride; sulfuric acid; oxygen;
In
1,4-dioxane; diethyl ether; dichloromethane; ethyl acetate;
DOI:10.1021/jm00087a020
