3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

Base Information

Chemical Name:3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester
CAS No.:149838-35-7
Molecular Formula:C₄₂H₆₄N₄O₁₂
Molecular Weight:816.99
Hs Code.:

3-<p-<(N-((tert-butoxycarbonyl)-γ-L-glutamyl-γ-L-glutamyl)-β-amino)ethyl>phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

Synonyms:3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

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Chemical Property of 3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

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Technology Process of 3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

There total 11 articles about 3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57732-63-5
1-tert-butyl 5-methyl (2S)-2-{[(benzyloxy)carbonyl]amino}pentanedioate

: 149838-35-7
3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 89 percent / H₂, 1 M methanolic HCl / 5percent Pd/C / 8 h

3: aq. NaOH

4: 88 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / Ambient temperature

5: 63 percent / aq. NaOH / methanol / 2 h / Ambient temperature

6: 85 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / Ambient temperature

7: 1.) aq. NaOH, 2.) dicyclohexylcarbodiimide (DCC), 4-(dimethylamino)pyridine / 1.) CH₃OH, RT, 2 h, 2.) CH₂Cl₂, RT, overnight

With hydrogenchloride; dmap; sodium hydroxide; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00068a022

Reference yield:

: 79640-72-5
L-glutamic acid 1-tert-butyl ester 5-methyl ester

: 149838-35-7
3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

Guidance literature:: Multi-step reaction with 6 steps

2: aq. NaOH

3: 88 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / Ambient temperature

4: 63 percent / aq. NaOH / methanol / 2 h / Ambient temperature

5: 85 percent / dicyclohexylcarbodiimide (DCC) / CH₂Cl₂ / Ambient temperature

6: 1.) aq. NaOH, 2.) dicyclohexylcarbodiimide (DCC), 4-(dimethylamino)pyridine / 1.) CH₃OH, RT, 2 h, 2.) CH₂Cl₂, RT, overnight

With dmap; sodium hydroxide; dicyclohexyl-carbodiimide; In methanol; dichloromethane;
DOI:10.1021/ja00068a022

Reference yield:

: 51-67-2
tyrosamine

: 149838-35-7
3-phenoxymethyl>-5-(((tert-butoxycarbonyl)amino)methyl)furan, di-tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 55 percent / aq. NaOH / dioxane / 1.5 h / 0 - 20 °C

2: KOH, n-Bu₄NBr / tetrahydrofuran / 3 h / Ambient temperature

3: n-Bu₄NF / tetrahydrofuran / 3 h / 50 °C

4: 1.) aq. NaOH, 2.) dicyclohexylcarbodiimide (DCC), 4-(dimethylamino)pyridine / 1.) CH₃OH, RT, 2 h, 2.) CH₂Cl₂, RT, overnight

With dmap; potassium hydroxide; sodium hydroxide; tetrabutyl ammonium fluoride; tetrabutylammomium bromide; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1021/ja00068a022